Manufacturer: Nomura Chemical Co., Ltd.India distributor: Akira Analytical Solutions Pvt. Ltd.

Application Note: Highly Polar Compound Analysis

Strategies for improving retention and peak shape for polar analytes.

This application note provides a method-development framework. Final conditions must be validated with the actual analytes, matrix, detector and laboratory system.

Why conventional C18 can struggle

Highly polar compounds may elute close to the solvent front on conventional C18, especially under water-rich conditions. An aqueous-compatible reversed-phase family can provide more stable retention.

Aqueous starting conditions

Begin with a high proportion of water and only enough organic modifier to maintain suitable peak shape and run time. Confirm that the selected phase is designed for water-rich operation.

pH and ionic form

Control pH to manage ionization and retention. Use an appropriate buffer where needed and verify compatibility with the detector, especially for LC–MS.

Alternative mode

When reversed-phase retention remains insufficient, evaluate a polar-retention mode such as HILIC within the Fusion portfolio, using careful control of water content and sample solvent.

Column selection

Recommended Develosil Starting Points

Fusion Columns

View product information, selection guidance and available configurations.

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